This week's imide synthesis involves two reactions. In the first reaction (24A), a(n) bond is formed between the two reactants. Hint: What type of functional group is formed

Straightforward questions answered in the powerpoint slidesreaction: heating the starting materials under refluxwhat does it mean to heat under reflux? why do we choose water as the reflux solvent? what are boiling chips used for? why do we put a condenser on top of the reaction? why do we add heat and let the reaction stir for 30 minutes? why do we add sulfuric acid to the reaction after it cools as opposed to when it’s still hot? separation: filtration of precipitatewhy don’t we do an aqueous and organic extraction in the separatory funnel? why do you rinse the salicylic acid on the filter with ice cold water? purification: recrystallization of salicylic acid (no hot filtration needed)what is the difference in the amount of room temperature water vs. boiling water needed to dissolve the salicylic acid (assume a 1.2 gram yield of salicylic acid)? remember, in the lab if you need x ml of boiling water to dissolve a solid, then you should add a little more (definitely no more than 1.5 times the theoretical amount) to ensure it doesn’t recrystallize prematurely.analysis: melting point of salicylic acidwhat can you conclude if the melting point of the salicylic acid you just synthesized is 152-155oc and the 1: 1 mix of your product and “synthetic” salicylic acid is 151-154oc?

Melissa is interested in her family tree and how her family has changed over its many generations. melissa probably more closely resembles

Americium-241 undergoes fission to produce three neutrons per fission event. if a neutron-absorbing material is mixed in with this sample so that the rate of neutron production drops down to 1.8 neutrons per fission event, which will be effective at achieving a critical mass? check all that apply. remove a deflective shield surrounding the sample. remove absorbent material mixed in with the sample. compress the sample of americium-241.