Step 5: Measure the Reaction Rate at = 5°C 10
150
100
-10
50
Once the temperature is measured, remove thermometer.
Temperature of the water:
°C. Reaction time:
seconds DONE
Intro

An aqueous solution of hydroiodic acid is standardized by titration with a 0.186 m solution of calcium hydroxide. if 26.5 ml of base are required to neutralize 20.3 ml of the acid, what is the molarity of the hydroiodic acid solution? m hydroiodic acid

Straightforward questions answered in the powerpoint slidesreaction: heating the starting materials under refluxwhat does it mean to heat under reflux? why do we choose water as the reflux solvent? what are boiling chips used for? why do we put a condenser on top of the reaction? why do we add heat and let the reaction stir for 30 minutes? why do we add sulfuric acid to the reaction after it cools as opposed to when it’s still hot? separation: filtration of precipitatewhy don’t we do an aqueous and organic extraction in the separatory funnel? why do you rinse the salicylic acid on the filter with ice cold water? purification: recrystallization of salicylic acid (no hot filtration needed)what is the difference in the amount of room temperature water vs. boiling water needed to dissolve the salicylic acid (assume a 1.2 gram yield of salicylic acid)? remember, in the lab if you need x ml of boiling water to dissolve a solid, then you should add a little more (definitely no more than 1.5 times the theoretical amount) to ensure it doesn’t recrystallize prematurely.analysis: melting point of salicylic acidwhat can you conclude if the melting point of the salicylic acid you just synthesized is 152-155oc and the 1: 1 mix of your product and “synthetic” salicylic acid is 151-154oc?

Which process describes vaporization that takes place below the surface of a liquid? condensation melting boiling evaporation